HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13021275, compound → Pregna-1,4-diene-3,11,20-trione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13021275 | HCID 13021275 | — |
| Reactant | Jones' reagent | HCID 131709961 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Pregna-1,4-diene-3,11,20-trione | HCID 247932 | — |
Reaction Steps
11α-Hydroxypregna-1,4-diene-3,20-dione (120 mmol) in acetone (950 ml) is treated with Jones reagent (38.7 ml) at 0°. Following work-up the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04996318 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-33b2f1b06d9b4b2aa92c99a6d4d0412f |
| Source note | uspto-grants-1991_02 |