HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylthiocarbamoyl chloride → HCID 20068261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| Reactant | HCID 20068242 | HCID 20068242 | — |
| Product | HCID 20068261 | HCID 20068261 | 90.1% |
Reaction Steps
Following the procedure described in Preparation I and starting from 13.3 g (0.059 mol) of 2-cyanophenyl 4-hydroxyphenyl methanone and 8.5 g (0.068 mol) of dimethylthiocarbamoyl chloride, 16.5 g (yield: 89%) of O-4-(2-cyanobenzoyl)phenyl dimethylthiocarbamate melting at 138° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04996347 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-6cd78ede72f4463aab6683e7853a9e41 |
| Source note | uspto-grants-1991_02 |