HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → Cyclododeca-3,7-dien-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 1,2-Epoxycyclododeca-5,9-diene | HCID 79135 | — |
| Product | Cyclododeca-3,7-dien-1-one | HCID 69032822 | 98.7% |
Reaction Steps
Also, German Patent DE3601380 discloses a technique where 1,2-epoxycyclododeca-5,9-diene is isomerized in the presence of sodium iodide in a polyethylene glycol solvent (NaI: 3 wt %, 195° C., 9 hours) and thereby cyclododeca-3,7-dien-1-one is produced in a yield of 98.7%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06861563B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-fac9e2f23c724e5fa1663ed79ad68599 |
| Source note | uspto-grants-2005_03 |