HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Methylthio)phenylacetic acid → N-[(3-methylthiophenyl)acetyl]alanine Iso-butyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Methylthio)phenylacetic acid | HCID 2737461 | — |
| Reactant | 2-methylpropyl (2S)-2-aminopropanoate | HCID 13743556 | — |
| Product | N-[(3-methylthiophenyl)acetyl]alanine Iso-butyl Ester | HCID 15481777 | — |
Reaction Steps
Following General Procedure I′ above, and using 3-methylthiophenylacetic acid (CAS# 18698-73-2) and alanine iso-butyl ester (prepared following General Procedure J′ above), the title compound was prepared. The reaction was m monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06861558B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-82ac25ad7e81450ea27ad950e4ab3d7e |
| Source note | uspto-grants-2005_03 |