HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → N-2-ethylhexyl-3,6-diformyl carbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | N-heptyl-3,6-Diformylcarbazole | HCID 11141782 | — |
| Reactant | N-2-Ethylhexylcarbazole | HCID 66872719 | — |
| Product | N-2-ethylhexyl-3,6-diformyl carbazole | HCID 86590067 | — |
Reaction Steps
N-2-ethylhexyl-3,6-diformyl carbazole was prepared from DMF (97 ml, 1.25 mol), POCl3 (116.5 ml, 1.25 mol), and N-2-ethylhexylcarbazole (50 g, 0.18 mol) according to the procedure described for N-heptyl-3,6-Diformylcarbazole. The product was obtained as 40 g of brownish liquid (66% yield). The product was used as is in the next step without any purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06864025B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-0b43e9d1255948f2ab0af6d383b895df |
| Source note | uspto-grants-2005_03 |