HCID 18604804, compound → HCID 178462255, compound

HRID 983509Notes

Reaction equation

HRID 983509 reaction equation
[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9].[NH2:13][C@H:14]([C:20](Cl)=[O:21])[CH2:15][CH2:16][CH2:17][CH2:18][NH2:19]>N1C=CC=CC=1>[NH2:13][C@H:14]([C:20]([OH:21])=[O:6])[CH2:15][CH2:16][CH2:17][CH2:18][NH2:19].[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9]

Participants

4

Reactant 2

HCID 18604804HCID 18604804, compoundHCID 178462254HCID 178462254, compound

Product 1

HCID 178462255HCID 178462255, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

6-Deoxyamino ascorbate (5 mmoles) is reacted with lysyl chloride (7 mmoles) in dry pyridine and the reaction product is worked up according to Cousine et al. It is crystallized from ethanol.

Workup

  1. customis crystallized from ethanol

Sources & evidence

ORD record
ord-f8c59478c02442fb9c53fa60fe82e18d
Source dataset
uspto-grants-2005_03
Patent number
US06864284B2

Reaction notes

Loading…