HCID 12378858, compound → HCID 178462256, compound

HRID 983510Notes

Reaction equation

HRID 983510 reaction equation
[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9].[NH:13]1CCC[C@H]1C(Cl)=O>N1C=CC=CC=1>[NH:13]1[CH2:10][CH2:2][CH2:3][C@H:4]1[C:5]([OH:7])=[O:6].[NH2:1][C@:2]1([C@H:10]([CH3:12])[OH:11])[O:7][C:5](=[O:6])[C:4]([OH:8])=[C:3]1[O-:9]

Participants

4

Reactant 2

HCID 12378858HCID 12378858, compoundHCID 178462254HCID 178462254, compound

Product 1

HCID 178462256HCID 178462256, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

6-Deoxyamino ascorbate (5 mmoles) is reacted with prolyl chloride (7 mmoles) in dry pyridine and worked up by the method as described above and crystallized from ethanol.

Workup

  1. customcrystallized from ethanol

Sources & evidence

ORD record
ord-020ee30b642248f690f035085c447098
Source dataset
uspto-grants-2005_03
Patent number
US06864284B2

Reaction notes

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