HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5,5-Trimethylhexanoylbenzene → 3,5,5-Trimethylhexylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5,5-Trimethylhexanoylbenzene | HCID 22269478 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3,5,5-Trimethylhexylbenzene | HCID 22269440 | — |
Reaction Steps
A solution of 116.5 grams of 3,5,5-Trimethylhexanoylbenzene in 1500 mL of tetrahydrofuran with 9.9 grams of 10% palladium on carbon (as a catalyst) was stirred at 23° C. in an atmosphere of hydrogen at 275 kPa for 17 hours. The mixture was filtered through Celite™ diatomaceous earth filter agent to remove the catalyst. The filtrate was concentrated in vacuo to give 3,5,5-trimethylhexylbenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06864396B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-680c9abc2d054d86bd99c72a778e4b12 |
| Source note | uspto-grants-2005_03 |