HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22557298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13604136 | HCID 13604136 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22557298 | HCID 22557298 | — |
Reaction Steps
10 mmol (2.2 g) of 4-(1,4,5,6-tetrahydro-6-oxo-3-pyridazinyl)benzoic acid are suspended in 50 ml of dichloromethane, after which 1.5 ml (20 mmol) of thionyl chloride are added and the mixture is stirred for 24 hours while being boiled gently.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867206B1 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-289c455c455f441f9a3cb3f6ba415f23 |
| Source note | uspto-grants-2005_03 |