2,4-Dichlorobenzylidenemalononitrile → HCID 10173422, compound

HRID 983839Notes

Reaction equation

HRID 983839 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[C:10]([C:12]([NH2:14])=[NH:13])[CH:9]=[C:8]2[C:4]=1[CH:5]=[CH:6][N:7]2[CH3:15].[Cl:16][C:17]1[CH:28]=[C:27]([Cl:29])[CH:26]=[CH:25][C:18]=1[CH:19]=[C:20]([C:23]#[N:24])[C:21]#[N:22]>>[NH2:24][CH2:23][C:20]1[C:21]([NH2:22])=[N:13][C:12]([C:10]2[CH:9]=[C:8]3[C:4]([CH:5]=[CH:6][N:7]3[CH3:15])=[C:3]([O:2][CH3:1])[CH:11]=2)=[N:14][C:19]=1[C:18]1[CH:25]=[CH:26][C:27]([Cl:29])=[CH:28][C:17]=1[Cl:16]

Participants

3

Reactant 2

HCID 180892,4-DichlorobenzylidenemalononitrileHCID 22220620HCID 22220620, compound

Product 1

HCID 10173422HCID 10173422, compound

Procedure

The title compound, MS: m/e=428.0 (M+H+), was prepared from 4-methoxy-1-methyl-1H-indole-6-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record
ord-cf9f1915a6744ebca54318f08dfbda8c
Source dataset
uspto-grants-2005_03
Patent number
US06867205B2

Reaction notes

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