2,4-Dichlorobenzylidenemalononitrile → HCID 10237507, compound
Reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[NH:7])=[CH:4][C:3]=1[O:11][CH3:12].[Cl:13][C:14]1[CH:25]=[C:24]([Cl:26])[CH:23]=[CH:22][C:15]=1[CH:16]=[C:17]([C:20]#[N:21])[C:18]#[N:19]>>[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]2[N:8]=[C:18]([NH2:19])[C:17]([CH2:20][NH2:21])=[C:16]([C:15]3[CH:22]=[CH:23][C:24]([Cl:26])=[CH:25][C:14]=3[Cl:13])[N:7]=2)=[CH:4][C:3]=1[O:11][CH3:12]Participants
3
Procedure
The title compound, MS: m/e=389.9 (M+H+), was prepared from 4-amino-3-methoxy-benzamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.
Sources & evidence
- ORD record
- ord-b51e3be894c64a2b87c9368fe3f3d942
- Source dataset
- uspto-grants-2005_03
- Patent number
- US06867205B2
Reaction notes
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