2,4-Dichlorobenzylidenemalononitrile → HCID 10149532, compound
Reaction equation
[CH3:1][O:2][C:3](=[NH:5])[NH2:4].[Cl:6][C:7]1[CH:18]=[C:17]([Cl:19])[CH:16]=[CH:15][C:8]=1[CH:9]=[C:10]([C:13]#[N:14])[C:11]#[N:12]>>[NH2:14][CH2:13][C:10]1[C:11]([NH2:12])=[N:5][C:3]([O:2][CH3:1])=[N:4][C:9]=1[C:8]1[CH:15]=[CH:16][C:17]([Cl:19])=[CH:18][C:7]=1[Cl:6]Participants
3
Procedure
The title compound, MS: m/e=337.8 (M+), was prepared from 2-methyl-isourea and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 a solid.
Sources & evidence
- ORD record
- ord-ea509412877f4ae48f7601427215b9cc
- Source dataset
- uspto-grants-2005_03
- Patent number
- US06867205B2
Reaction notes
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