2,4-Dichlorobenzylidenemalononitrile → HCID 10287238, compound

HRID 983863Notes

Reaction equation

HRID 983863 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([F:11])[CH:10]=1)[C:5]([NH2:7])=[NH:6].[Cl:12][C:13]1[CH:24]=[C:23]([Cl:25])[CH:22]=[CH:21][C:14]=1[CH:15]=[C:16]([C:19]#[N:20])[C:17]#[N:18]>>[NH2:20][CH2:19][C:16]1[C:17]([NH2:18])=[N:6][C:5]([C:4]2[CH:3]=[C:2]([F:1])[CH:10]=[C:9]([F:11])[CH:8]=2)=[N:7][C:15]=1[C:14]1[CH:21]=[CH:22][C:23]([Cl:25])=[CH:24][C:13]=1[Cl:12]

Participants

3

Reactant 2

HCID 180892,4-DichlorobenzylidenemalononitrileHCID 36907683,5-Difluoro-benzamidine

Product 1

HCID 10287238HCID 10287238, compound

Procedure

The title compound, MS: m/e=380.9 (M+H+), was prepared from 3,5-difluorobenzamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record
ord-1f10653162434e5eb4cade301047a244
Source dataset
uspto-grants-2005_03
Patent number
US06867205B2

Reaction notes

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