2,4-Dichlorobenzylidenemalononitrile → HCID 10216171, compound
Reaction equation
[S:1]1[C:5]([C:6]([NH2:8])=[NH:7])=[CH:4][C:3]2[CH:9]=[CH:10][CH:11]=[CH:12][C:2]1=2.[Cl:13][C:14]1[CH:25]=[C:24]([Cl:26])[CH:23]=[CH:22][C:15]=1[CH:16]=[C:17]([C:20]#[N:21])[C:18]#[N:19]>>[NH2:21][CH2:20][C:17]1[C:18]([NH2:19])=[N:7][C:6]([C:5]2[S:1][C:2]3[CH:12]=[CH:11][CH:10]=[CH:9][C:3]=3[CH:4]=2)=[N:8][C:16]=1[C:15]1[CH:22]=[CH:23][C:24]([Cl:26])=[CH:25][C:14]=1[Cl:13]Participants
3
Procedure
The title compound, MS: m/e=400.9 (M+H+), was prepared from benzo[b]thiophene-2-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.
Sources & evidence
- ORD record
- ord-43a7bbe61bfc4d1e8492d89e3607f69a
- Source dataset
- uspto-grants-2005_03
- Patent number
- US06867205B2
Reaction notes
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