2,4-Dichlorobenzylidenemalononitrile → HCID 10194700, compound

HRID 983867Notes

Reaction equation

HRID 983867 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]([NH2:15])=[NH:14])[CH:7]=[CH:6]2.[Cl:16][C:17]1[CH:28]=[C:27]([Cl:29])[CH:26]=[CH:25][C:18]=1[CH:19]=[C:20]([C:23]#[N:24])[C:21]#[N:22]>>[NH2:24][CH2:23][C:20]1[C:21]([NH2:22])=[N:14][C:13]([C:8]2[CH:7]=[CH:6][C:5]3[C:10](=[CH:11][CH:12]=[C:3]([O:2][CH3:1])[CH:4]=3)[CH:9]=2)=[N:15][C:19]=1[C:18]1[CH:25]=[CH:26][C:27]([Cl:29])=[CH:28][C:17]=1[Cl:16]

Participants

3

Procedure

The title compound, MS: m/e=425.0 (M+H+), was prepared from 6-methoxy-naphthalene-2-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record
ord-19b7d84c4b1d41d4bd9843342f2fb8a8
Source dataset
uspto-grants-2005_03
Patent number
US06867205B2

Reaction notes

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