HCID 22557739, compound → HCID 22557774, compound
Reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][C:10]=1[N:16]([C:24]([O:26]C(C)(C)C)=[O:25])[S:17]([CH2:20]CCC)(=[O:19])=[O:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(O)(=O)C.[CH2:35](OC1C=CC=CC=1N(C(OC(C)(C)C)=O)S(CCCC)(=O)=O)[C:36]1[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=1>>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][C:10]=1[N:16]([C:24]([O:26][CH2:35][C:36]1[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=1)=[O:25])[S:17]([CH3:20])(=[O:19])=[O:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
By carrying out the operation as described in preparation 13c but using the product from the preceding stage instead of the product from preparation 13b, the title compound is obtained.
Sources & evidence
- ORD record
- ord-bd2adf5090924cd196deed42caaf67cd
- Source dataset
- uspto-grants-2005_03
- Patent number
- US06867220B2
Reaction notes
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