HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,6-Dimethoxyphenyl)boronic acid → HCID 22557551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,6-Dimethoxyphenyl)boronic acid | HCID 2734343 | — |
| Reactant | (E)-ethyl 3-(4-bromophenyl)-but-2-enoate | HCID 15933615 | — |
| Product | HCID 22557551 | HCID 22557551 | 73% |
Reaction Steps
(E)-Ethyl 3-(2′,6′-dimethoxy-biphenyl-4-yl)-but-2-enoate (1.02 g, 73% yield) was prepared from 2,6-dimethoxyphenylboronic acid (1.20 g, 6.60 mmol) and (E)-ethyl 3-(4-bromophenyl)-but-2-enoate (1.0 g, 4.40 mmol) by a procedure analogous to that described in example 52 a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867218B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-edd880b663c04e14bfea090be4978850 |
| Source note | uspto-grants-2005_03 |