HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → (E)-3-(2',5'-dimethoxy-biphenyl-4-yl)-but-2-en-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | (E)-ethyl 3-(2',5'-dimethoxy-biphenyl-4-yl)-but-2-enoate | HCID 22557594 | — |
| Product | (E)-3-(2',5'-dimethoxy-biphenyl-4-yl)-but-2-en-1-ol | HCID 69796389 | — |
Reaction Steps
The colourless gum (E)-3-(2′,5′-dimethoxy-biphenyl-4-yl)-but-2-en-1-ol was prepared by DIBAL-H reduction of (E)-ethyl 3-(2′,5′-dimethoxy-biphenyl-4-yl)-but-2-enoate by a procedure analogous to that described in example 52b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867218B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-d287f7214325432caf43a9c1346fde23 |
| Source note | uspto-grants-2005_03 |