HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl (2S)-2-ethoxy-3-(4-hydroxyphenyl)propanoate → HCID 86589965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl (2S)-2-ethoxy-3-(4-hydroxyphenyl)propanoate | HCID 9816147 | — |
| Reactant | HCID 22557705 | HCID 22557705 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86589965 | HCID 86589965 | 73.3% |
Reaction Steps
The title compound (732 mg, 70%) was prepared as a yellow gum, (containing 0.25 molar equivalents of ethyl acetate) from (E)-3-(3′,5′-dichloro-biphenyl-4-yl)-prop-2-en-1-ol (559 mg, 2.0 mmol) and (S)-ethyl 2-ethoxy-3-(4-hydroxyphenyl)-propionate (500 mg, 2.10 mmol) by a procedure analogous to that described in example 52c.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867218B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-6b98357e367542d08aa7a0d441e812c1 |
| Source note | uspto-grants-2005_03 |