Indole → HCID 10791428, compound

Participants

Reaction Steps

The title compound was prepared by the procedures described in Example 217, substituting the indole from Example 186 with the indole from Example 85, resulting in a white solid. 1H NMR (CDCl3, 300 MHz) δ 2.15 (s, 3H), 2.54 (s, 6H), 3.47-3.85 (m, 8H), 4.05 (s, 2H), 6.56 (d, J=8.7 Hz, 1H), 6.77 (d, J=15.6 Hz, 1H), 7.09 (d, J=8.7 Hz, 1H), 7.36 (dd, J=1.5, 8.7 Hz, 1H), 7.50 (d, J=8.7 Hz, 1H), 7.52 (s, 2H), 7.56 (d, J=15.6 Hz, 1H), 7.88 (s, 1H), 9.27 (s, 1H). MS (ESI+) (M+H)+ at m/z 497, 499. Anal. Calcd for C26H29ClN4O2S.0.46 TFA.1.72 MeOH: C, 56.89; H, 6.06; N, 9.27. Found: C, 56.83; H, 6.15; N, 9.46.

Provenance & Evidence