HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexylamine → HCID 9964411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexylamine | HCID 8102 | — |
| Reactant | Benzene, 1-bromo-3,5-dimethyl- | HCID 136357 | — |
| Product | HCID 9964411 | HCID 9964411 | 91.1% |
Reaction Steps
Using the general procedure, 5-bromo-m-xylene (136 μL, 1.0 mmol) was coupled with n-hexylamine (198 μL, 1.5 mmol). Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (20:1) as eluent afforded the desired product as a colorless oil (187 mg, 91% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06867298B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-de4473302cd7417dae2ad561f98a49b1 |
| Source note | uspto-grants-2005_03 |