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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 984673Generated: October 31, 2026

4-Bromotoluene → HCID 9834366, compound

https://huagongshe.com/reaction/984673

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-BromotolueneHCID 7805—
Reactant2-(1-Cyclohexenyl)ethylamineHCID 76938—
ProductHCID 9834366HCID 983436695.2%

Reaction Steps

Using the general procedure, 4-bromotoluene (172 mg, 1.0 mmol) was coupled with 2-(1-cyclohexenyl)ethylamine (209 μL, 1.5 mmol). Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (20:1) as eluent afforded the desired product as a colorless oil (205 mg, 95% yield). Rf=0.6 (hexane/ethyl acetate=10:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06867298B2
Source datasetuspto-grants-2005_03
ORD IDord-a92114afb35f4a18963ceab0b73e25c2
Source noteuspto-grants-2005_03