HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → 7-Benzyl-8-bromo-3-methyl-1-(2-oxo-2-phenylethyl)-3,7-dihydropurine-2,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 7-Benzyl-8-bromo-3-methylxanthine | HCID 836152 | — |
| Product | 7-Benzyl-8-bromo-3-methyl-1-(2-oxo-2-phenylethyl)-3,7-dihydropurine-2,6-dione | HCID 22508576 | — |
Reaction Steps
7-Benzyl-8-bromo-3-methyl-3,7-dihydropurine-2,6-dione (77A) and 2-bromoacetophenone were reacted and purified as described in the General procedure G, Step B, to afford 77B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06869947B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-c85bc24fc06b4224ac0ad33bb1c4009e |
| Source note | uspto-grants-2005_03 |