2,5-Dimethylphenol → Ethyl 2,5-dimethylphenoxyacetate

HRID 985054Notes

Reaction equation

HRID 985054 reaction equation
[CH2:1]([O:3][C:4](=[O:14])[CH2:5][O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH3:13])[CH3:2].[CH3:15]C1C=CC(C)=CC=1O>>[CH2:1]([O:3][C:4](=[O:14])[CH2:5][O:6][C:7]1[CH:12]=[C:11]([CH3:15])[CH:10]=[CH:9][C:8]=1[CH3:13])[CH3:2]

Participants

3

Reactant 2

HCID 72672,5-DimethylphenolHCID 3022879Ethyl 2-(2-methylphenoxy)acetate

Product 1

HCID 17065224Ethyl 2,5-dimethylphenoxyacetate

Procedure

The title compound was prepared according to the method described for preparing compound 10.1, using 2,5-dimethylphenol as the starting material. 1H NMR (400 MHz) (CDCl3) δ 7.03 (1H, d, J=7.5 Hz); 6.72 (1H, d, J=7.5 Hz); 6.52 (1H, s); 4.62 (2H, s); 4.27 (2H, q, J=7.1 Hz); 2.30 (3H, s); 2.25 (3H,s); 1.30 (3H, t, J=7.1 Hz).

Sources & evidence

ORD record
ord-e633cfb793974213ad1f55d45160717a
Source dataset
uspto-grants-2005_03
Patent number
US06869975B2

Reaction notes

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