HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → Methanimidic acid, N-phenyl-, ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | N,N'-Diphenylformamidine | HCID 94888 | — |
| Product | Methanimidic acid, N-phenyl-, ethyl ester | HCID 111236 | — |
Reaction Steps
The synthesis is achieved in three steps. The first step is the preparation of N,N′-diphenyl formamidine (by the reaction of aniline with triethyl orthoformate). This intermediate is then further reacted with triethyl orthoformate to produce ethyl N-phenylimidoformate. The final step is the reaction of ethyl phenylimidoformate with 4-aminostyrene to give the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06870021B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-1c6e210e535a4897a7e342566cd491a7 |
| Source note | uspto-grants-2005_03 |