HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 20767931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 1,2-dimethyl-6-methoxy1H-indole-3-carboxylic acid | HCID 22143494 | — |
| Product | HCID 20767931 | HCID 20767931 | — |
Reaction Steps
This material was prepared from 1,2-dimethyl-6-methoxy-1H-indole-3-carboxylic acid 16c, oxalyl chloride and isopropylamine in a manner as previously described for example 16d. 1H NMR (300 MHz, CDCl3) δ7.53 (1H, d, J=8.7 Hz), 6.85 (1H, dd, J=2.3, 8.7 Hz), 6.77 (1H, d, J=2.3 Hz), 4.35 (1H, m), 3.87 (3H, s), 3.63 (3H, s), 2.69 (3H, s), 1.30 (3H, s), 1.27 (3H, s). LCMS (ESI+) [M+]H/z Calc'd 261, found 261.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06869962B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-bf7455bb435c43a4948f730c2849699d |
| Source note | uspto-grants-2005_03 |