HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 11333276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 69312246 | HCID 69312246 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11333276 | HCID 11333276 | — |
Reaction Steps
The above product of step 2 was dissolved in 100 mL methylene chloride and treated with 12 mL TFA. After stirring overnight, the volatiles were removed and the product crystallized from 10:1 methylene chloride/MeOH. In this way 8.0 g of 6-methanesulfonyl-2-methyl-1H-indole was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06872744B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-c9b571d9f7d94f89a58b60de8e2613b2 |
| Source note | uspto-grants-2005_03 |