HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 86594664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | (+)-(7-[1,4]Dioxan-2-yl-4-methoxy-benzothiazol-2-yl)-carbamic acid phenyl ester | HCID 20769454 | — |
| Reactant | (4-Methyl-piperidin-4-yl)-methanol trifluoroacetate | HCID 22507736 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86594664 | HCID 86594664 | — |
Reaction Steps
From (+)-(7-[1,4]dioxan-2-yl-4-methoxy-benzothiazol-2-yl)-carbamic acid phenyl ester with (4-methyl-piperidin-4-yl)-methanol trifluoroacetate and N-ethyldiisopropylamine in chloroform [α]D20=+24.1° (c=1.02, CHCl3), ES-MS m/e (%): 422 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06872833B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-0a4e8d4cec244106a591e3b4ae81bda2 |
| Source note | uspto-grants-2005_03 |