HCID 20075285, compound → HCID 20075273, compound

HRID 985920Notes

Reaction equation

HRID 985920 reaction equation
NC1C=CC(C2C=C(C)C=CC=2S(C2C=CC(C)=CC=2C2C=CC(N)=C([N+]([O-])=O)C=2)=O)=CC=1[N+]([O-])=O.[CH2:37]([NH:39][C:40]1[CH:45]=[CH:44][C:43]([S:46]([C:48]2[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=2)=[O:47])=[CH:42][C:41]=1[N+:54]([O-])=O)[CH3:38]>>[NH2:54][C:41]1[CH:42]=[C:43]([S:46]([C:48]2[CH:49]=[CH:50][CH:51]=[CH:52][CH:53]=2)=[O:47])[CH:44]=[CH:45][C:40]=1[NH:39][CH2:37][CH3:38]

Participants

3

Reactant 2

HCID 20075285HCID 20075285, compoundHCID 53642139(4-Amino-3-nitrophenyl)-4-methylphenyl sulfoxide

Product 1

HCID 20075273HCID 20075273, compoundYield 93%

Procedure

Following the procedure described in Example 40 but using as a starting material instead of (4-amino-3-nitrophenyl)-4-methylphenyl sulfoxide a corresponding amount of (4-ethylamino-3-nitrophenyl)-phenyl sulfoxide, the title compound is obtained.

Sources & evidence

ORD record
ord-9cc8de36adbd4112b221d01085df83cd
Source dataset
uspto-grants-1987_12
Patent number
US04710323

Reaction notes

Loading…