Sodium bis(2-methoxyethoxy)aluminiumhydride → HCID 70390929, compound

Participants

Reaction Steps

A mixture of 0.125 g (0.43 mmol) of (2RS, 10bSR)-N-methyl-2-(2-methylamino-1,3,4,6,7,10b-hexahydrothieno[2,3-a]quinolizin-2-yl)acetamide and 0.51 ml (1.72 mmol) of 3.4 M sodium bis (2-methoxyethoxy) aluminum hydride were reacted employing the procedure substantially described in Example 27 Step B to give 0.07 g (59%) of (2RS,10bSR)-2-methylamino-2-(2-methylaminoethyl)-1,3,4,6,7,10b-hexahydrothieno[2,3-a]quinolizine as a brown oil.

Provenance & Evidence