Ethanol → HCID 13230948, compound

Participants

Reaction Steps

15 g of N-acetyl-D-glucosamine and 18.8 g of octadecylamine were heated at 80° C. in 50 ml of ethanol for 3 hours, with stirring. The undissolved material was then filtered off hot, the filtrate was cooled and the product which had precipitated was filtered off with suction and washed with ethanol and ether.2.2 g of the 2-acetamido-2-deoxy-N-octadecyl-glucopyranosylamine thus obtained were stirred in 17 ml of THF with 2 g of sodium carbonate. 1.45 g of oleoy) chloride in 5 ml of THF were then added dropwise.

Provenance & Evidence