Octadecylamine → HCID 18608592, compound

HRID 985972Notes

Reaction equation

HRID 985972 reaction equation
O=[CH:2][C@H:3]([C@@H:5]([C@@H:7]([C@H:9]([CH3:11])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:12]([NH2:30])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>C(O)C>[CH2:12]([NH:30][CH:11]1[O:4][C@@H:3]([CH3:2])[C@@H:5]([OH:6])[C@@H:7]([OH:8])[C@@H:9]1[OH:10])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

4

Reactant 2

HCID 15793OctadecylamineHCID 3034656L-(-)-Fucose

Product 1

HCID 18608592HCID 18608592, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3.26 g of L-fucose and 5.38 g of stearylamine were heated at 70° C. in 20 ml of ethanol, with stirring, until a clear solution had formed. The solution was allowed to cool and, when crystallization had ended, the solid was filtered off with suction and washed with ethanol and ether.

Workup

  1. customhad formed
  2. temperatureto cool
  3. customwhen crystallization
  4. filtrationthe solid was filtered off with suction
  5. washwashed with ethanol and ether

Sources & evidence

ORD record
ord-d3a27fdfd1ef4366b12bb7be9b76bb8b
Source dataset
uspto-grants-1987_12
Patent number
US04710491

Reaction notes

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