Tributyltin azide → HCID 20158968, compound

Participants

Reaction Steps

6-Cyano-2-methoxyquinoline (0.368 g) and tri-n-butyltin azide (0.73 g) were heated together at 110° for 18 hours to afford 2-methoxy-6-(1-tributylstannyl-(1H)-tetrazol-5-yl)quinoline as a crude oil which was not purified further but was used directly in the preparation of 6-(tetrazol-5-yl)-2-(1H)-quinolone (see Example 43).

Provenance & Evidence