HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 6-{2-[6-[(4-acetoxyphenyl)methoxy]-2,4-dichlorophenyl]ethyl}-3,4,5,6-tetrahydro-4-hydroxy-2H-pyran-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 2,4-Dichloro-6-hydroxybenzaldehyde | HCID 528390 | — |
| Reactant | 4-(Bromomethyl)phenyl acetate | HCID 10998771 | — |
| Reactant | 6-{2-(2,4-Dichloro-6-hydroxyphenyl)-ethyl}-3,4,5,6-tetrahydro-4-hydroxy-2H-pyran-2-one | HCID 13553196 | — |
| Product | 6-{2-[6-[(4-acetoxyphenyl)methoxy]-2,4-dichlorophenyl]ethyl}-3,4,5,6-tetrahydro-4-hydroxy-2H-pyran-2-one | HCID 20159037 | — |
Reaction Steps
By following the procedure of Example 1, Step A, but substituting equimolar amounts of 6-[2-(2,4-dichloro-6-hydroxyphenyl)ethyl]-3,4,5,6-tetrahydro-4-hydroxy-2H-pyran-2-one and 4-(bromomethyl)phenol acetate for the 4,6-dichlorosalicylaldehyde and benzyl bromide used therein, the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04710513 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-7e162731d3ad4639a60801b59a2a19ad |
| Source note | uspto-grants-1987_12 |