HRID986100

反应详情

EQUATION

反应方程式

HRID 986100 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A flask was charged with 23.37 g of optically active 4-benzyloxyphenyl 6-methyloctyl ether, 2.33 g of 10% Pd/C and 230 ml of ethanol, and the mixture was reacted at room temperature until it reacted with a theoretical amount of hydrogen. After completion of the reaction, the catalyst was removed by filtration and the organic solvent was distilled under reduced pressure to obtain a crude product. The crude product was refined to obtain 16.91 g of the intended phenol.

WORKUP

后处理

  1. customthe mixture was reacted at room temperature until it
  2. customAfter completion of the reaction
  3. customthe catalyst was removed by filtration
  4. distillationthe organic solvent was distilled under reduced pressure
  5. customto obtain a crude product