反应详情

温度

60 °C

In 10 ml of pyridine was dissolved 4.0 g of 1,3-propanediol monotosylate and the mixture was stirred at 60° C. overnight. The mixture was concentrated under reduced pressure to give the desired compound as a colorless oily material. Yield: 5.6 g (quantitative).

1. concentrationThe mixture was concentrated under reduced pressure