Diethyl Ether → HCID 13917420, compound

Participants

Reaction Steps

To a solution of 650 mg (1.42 mmols) of 1α,3β-diacetoxychol-5-en-24-ol in 35 ml of methylene chloride was added 750 mg (3.48 mmols) of pyridinium chlorochromate, and the resulting mixture was stirred at room temperature for 2 hours. Subsequently, 100 ml of ether was added to the mixture and the solution was eluted through a column filled with 15 g of Florisil to give 550 mg of 1α,3β-diacetoxychol-5-en-24-al (Compound B).

Provenance & Evidence