N-Ethyl-sec-butylamine → HCID 13336347, compound

HRID 986268Notes

Reaction equation

HRID 986268 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:17]=[C:16]([C:18]([OH:20])=O)[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[N:9]=1.[CH2:21]([NH:23][CH:24]([CH2:26][CH3:27])[CH3:25])[CH3:22]>S(Cl)(Cl)=O>[CH2:21]([N:23]([CH:24]([CH3:25])[CH2:26][CH3:27])[C:18]([C:16]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[N:9]=[C:8]([C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[Cl:1])[CH:17]=1)=[O:20])[CH3:22]

Participants

4

Reactant 2

HCID 89416N-Ethyl-sec-butylamineHCID 2691712-(2-chlorophenyl)quinoline-4-carboxylic acid

Product 1

HCID 13336347HCID 13336347, compound

Reagents, catalysts & solvents 1

HCID 24386Thionyl ChlorideSolvent

Procedure

The procedure of Example 3 is followed using 2-(2-chlorophenyl)-quinoline-4-carboxylic acid (2.8 g), thionyl chloride (10 ml) and N-ethylbut-2-ylamine (4 g) as the starting materials.

Sources & evidence

ORD record
ord-b6f8d8faa3934a368754b82f016022c8
Source dataset
uspto-grants-1987_12
Patent number
US04711890

Reaction notes

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