HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Pyroglutamic Acid → HCID 14369414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Pyroglutamic Acid | HCID 7405 | — |
| Reactant | Carbodiimide | HCID 160435 | — |
| Reactant | HCID 14369442 | HCID 14369442 | — |
| Product | HCID 14369414 | HCID 14369414 | 82% |
Reaction Steps
Pyroglutamyl-glycyl-glycyl-seryl-asparaginyl-phenylalanine 2-phenylethylamide is prepared from pyroglutamic acid and glycyl-glycyl-seryl-asparaginyl-phenylalanine 2-phenylethylamide using the carbodiimide method similar to that described in the preceding example 5. Yield 82 %, m.p. 209°-211° C., Rf 0.25/S1, 0.67/S2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04711952 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-26c03ad87ab8456297fb509b9575e681 |
| Source note | uspto-grants-1987_12 |