4-Methylmorpholine → HCID 118641978, compound

Participants

Reaction Conditions

Reaction Steps

NMM (0.4 g, 4 mmol) and isobutylchloroformate (0.53 g, 4 mmol) are added to the obtained solution, cooled to -15° C. and kept under nitrogen atmosphere and, two minutes later, a DMF solution of Lys(Boc)-PheNH2 (1.6 g, 4 mmol), obtained by cleavage of the benzyloxycarbonyl group from Z-Lys(Boc)-PheNH2 through catalytic hydrogenation over 10% Pd-on-carbon, is added.

Provenance & Evidence