HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86741940, compound → Ethyl 3-[4-(pyridin-3-yloxy)phenyl]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86741940 | HCID 86741940 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-[4-(pyridin-3-yloxy)phenyl]propionate | HCID 20148644 | 99% |
Reaction Steps
In 20 ml of ethanol was dissolved 2.0 g of ethyl (E)-3-[4-(pyridin-3-yloxy)phenyl]acrylate, and to the resulting solution was added 1.0 g of 5% palladiumcarbon, after which the resulting mixture was stirred in a hydrogen atmosphere at room temperature for 5 hours. The reaction mixture was filtered and the filtrate thus obtained was concentrated under reduced pressure to obtain 2.0 g (yield 99%) of colorless, oily ethyl 3-[4-(pyridin-3-yloxy)phenyl]propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04713387 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-a30f77edf86449639f06788431823da9 |
| Source note | uspto-grants-1987_12 |