Diethyl Ether → HCID 13151638, compound

HRID 986470Notes

Reaction equation

HRID 986470 reaction equation
[CH2:1]([N:3]1[C:12](=[O:13])[C:11]2[N:10]([CH2:14][CH2:15][CH2:16][CH2:17][CH:18]=[CH2:19])[CH:9]=[N:8][C:7]=2[N:6]([CH2:20][CH3:21])[C:4]1=[O:5])[CH3:2].C([O:24]CC)C>[Os](=O)(=O)(=O)=O>[CH2:1]([N:3]1[C:12](=[O:13])[C:11]2[N:10]([CH2:14][CH2:15][CH2:16][CH2:17][CH:18]3[O:24][CH2:19]3)[CH:9]=[N:8][C:7]=2[N:6]([CH2:20][CH3:21])[C:4]1=[O:5])[CH3:2]

Participants

4

Reactant 2

HCID 3283Diethyl Ether2×HCID 20157773HCID 20157773, compound

Product 1

HCID 13151638HCID 13151638, compound

Reagents, catalysts & solvents 1

HCID 30318Osmium TetroxideCatalyst2×

Procedure

The same compound was also obtained by hydroxylation of 1,3-diethyl-7-(5-hexenyl)xanthine ##STR19## with osmium tetroxide: 0.73 g of 1,3-diethyl-7-(5-hexenyl)xanthine in 11 ml of diethyl ether was added dropwise with stirring in 5 minutes to 0.65 g of osmium tetroxide in 11 ml of diethyl ether at room temperature.

Sources & evidence

ORD record
ord-4d8e4a910df9402d8aaa78cb7bff2c00
Source dataset
uspto-grants-1987_12
Patent number
US04713455

Reaction notes

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