Benzyl 4-Hydroxybenzoate → HCID 13822729, compound

HRID 986519Notes

Reaction equation

[OH:1][C:2]1[CH:17]=[CH:16][C:5]([C:6]([O:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[O:7])=[CH:4][CH:3]=1.[C:18](Cl)(=[O:25])[CH2:19][CH2:20][CH2:21][C:22](Cl)=[O:23]>>[CH2:9]([O:8][C:6]([C:5]1[CH:16]=[CH:17][C:2]([O:1][C:18](=[O:25])[CH2:19][CH2:20][CH2:21][C:22]([O:1][C:2]2[CH:3]=[CH:4][C:5]([C:6]([O:8][CH2:9][C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=3)=[O:7])=[CH:16][CH:17]=2)=[O:23])=[CH:3][CH:4]=1)=[O:7])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

Reactant 2

HCID 7180Benzyl 4-Hydroxybenzoate

HCID 17887Pentanedioyl dichloride

Product 1

HCID 13822729HCID 13822729, compound

Procedure

A similar procedure to Example 1 is carried out by using 22.8 g of benzyl p-hydroxybenzoate and 8.45 g of glutaric acid dichloride to yield di(p-benzyloxycarbonylphenyl)glutarate, m.p. 93°-94° C., as white crystals.

Sources & evidence

ORD record: ord-9abf9a34c7d14187ac40a03d8007c102
Source dataset: uspto-grants-1987_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04713474

Reaction notes

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