HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl phenylacetate → Potassium phenylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl phenylacetate | HCID 7559 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Product | Potassium phenylacetate | HCID 23675783 | 92% |
Reaction Steps
Under the reaction conditions described in Example 1, 64 ml KOH and 19.2 ml PPh3 were added over 43 min. After five more minutes, the reactor was cooled and vented. A 92% yield of potassium phenylacetate and 4% methyl phenylacetate was obtained on a nearly quantitative conversion. 98% of the stiochiometric amount of KOH was added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04713484 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-c38081a5ab9d4ffd80dd12009f8cf9bf |
| Source note | uspto-grants-1987_12 |