HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 3-(3-bromophenyl)prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 3-(3-Bromophenyl)acrylic acid | HCID 36251 | — |
| Product | Methyl 3-(3-bromophenyl)prop-2-enoate | HCID 610698 | 81% |
Reaction Steps
Reaction of 3-bromocinnamic acid (22.72 g) with methyl lodide (21.3 g) as described in Example 1 gave the title ester (19.5 g, 81%) as a white solid mp (methanol) 62°-65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04713486 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-b7f362e3364b4862b14137fe333145c8 |
| Source note | uspto-grants-1987_12 |