Sodium Hydroxide → HCID 23673130, compound

HRID 986567Notes

Reaction equation

HRID 986567 reaction equation
[CH3:1][N:2]1[C:10]([CH3:11])=[CH:9][C:8](=[O:12])[C:4]([C:5]([OH:7])=[O:6])=[C:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[OH-].[Na+:20]>CO>[CH3:1][N:2]1[C:10]([CH3:11])=[CH:9][C:8](=[O:12])[C:4]([C:5]([O-:7])=[O:6])=[C:3]1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[Na+:20]

Participants

4

Reactant 2

HCID 14798Sodium Hydroxide2×HCID 14075272HCID 14075272, compound

Product 1

HCID 23673130HCID 23673130, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.69 g of 1,6-dimethyl-2-phenyl-4-oxonicotinic acid is suspended in approximately 50 ml of methanol. NaOH pellets (0.305 gms) are added with stirring. After both the acid and the sodium hydroxide dissolve the solution is evaporated to dryness in vacuo. Sodium 1,6-dimethyl-2-phenyl-4-oxonicotinate is then isolated as a glossy, somewhat hydroscopic solid. Yield=1.6 g.

Workup

  1. customis evaporated to dryness in vacuo

Sources & evidence

ORD record
ord-32af6153bca845b1b9429dd4cf9ad097
Source dataset
uspto-grants-1987_12
Patent number
US04714492

Reaction notes

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