Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Silicon carbide → 1,2,4-Trimethoxy-5-nitrobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Silicon carbide | HCID 9863 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-Chloro-4,5-dimethoxy-2-nitrobenzene | HCID 12321273 | — |
| 생성물 | 1,2,4-Trimethoxy-5-nitrobenzene | HCID 822415 | — |
반응 단계
Into a two liter flask, provided with a cooling device, were introduced successively a solution of methanolic potash (100 g of KOH and 500 cm3 of methanol), then 100 g (0.46 mole) of 4,5-dimethoxy 2-nitro chlorobenzene and carborundum. The mixture was brought to boiling under reflux for 6 h. After cooling, the reaction medium was filtered; the precipitate obtained was washed with methanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04714700 |
| 출처 데이터셋 | uspto-grants-1987_12 |
| ORD ID | ord-baa8f31480994247bd915526e8860d87 |
| 출처 메모 | uspto-grants-1987_12 |