HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → HCID 13376465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | HCID 13376457 | HCID 13376457 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13376465 | HCID 13376465 | 84.4% |
Reaction Steps
3.5 g of N-(2-fluoroacetamido-5-nitrobenzoyl)-2,3-dimethylaniline, 3.0 g of boron trifluoride etherate and 30 ml of acetic acid are treated in the same manner as described in Example 1-(2), whereby 2.8 g of 2-fluoromethyl-3-(2,3-dimethylphenyl)-6-nitro-4(3H)-quinazolinone are obtained as yellow prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04714702 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-dd67a7c5f68c43f884ab77efa93648db |
| Source note | uspto-grants-1987_12 |