HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Fluoroacetyl chloride → N-(2-fluoroacetamido-5-nitrobenzoyl)-2-methyl-4-fluoroaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Fluoroacetyl chloride | HCID 9663 | — |
| Edukt | HCID 13376450 | HCID 13376450 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | N-(2-fluoroacetamido-5-nitrobenzoyl)-2-methyl-4-fluoroaniline | HCID 13376458 | 84,9% |
Reaktionsschritte
3.9 g of N-(2-amino-5-nitrobenzoyl)-2-methyl-4-fluoroaniline, 1.6 g of pyridine and 1.96 g of fluoroacetyl chloride are treated in the same manner as described in Example 1-(1), whereby 4.0 g of N-(2-fluoroacetamido-5-nitrobenzoyl)-2-methyl-4-fluoroaniline are obtained as colorless needles.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04714702 |
| Quelldatensatz | uspto-grants-1987_12 |
| ORD ID | ord-f34f851317ce42428e32186aebcd1f37 |
| Quellennotiz | uspto-grants-1987_12 |