HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → HCID 12593158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | HCID 12593153 | HCID 12593153 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12593158 | HCID 12593158 | 94.1% |
Reaction Steps
4.0 g of N-(2-fluoroacetamido-5-nitrobenzoyl)-2-methyl-4-bromoaniline, 3.0 g of boron trifluoride etherate and 30 ml of acetic acid are treated in the same manner as described in Example 1-(2), whereby 3.6 g of 2-fluoromethyl-3-(2-methyl-4-bromophenyl)-6-nitro-4(3H)-quinazolinone are obtained as pale yellow prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04714702 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-7cb063a8081d4110986beb7a2ddbd26e |
| Source note | uspto-grants-1987_12 |